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Visuals for Basic NMR Training Workshop Lecture I

These visuals are made from the original lecture transparencies

  •    The Rules
  •    NMR Instruments in the Facility
  •    Gemini-200 R2D2 Magnet
  •    Gemini-200 Console and Cockpit
  •    Unity-300 Magnet and Autosampler
  •    Unity-300 Console and Cockpit
  •    Avance-III-400 Magnet and Autosampler
  •    Avance-III-400 Console and Cockpit
  •    Avance-III-400 SampleJet Carousel
  •    DRX-500 Magnet and Console
  •    DRX-500 Cockpit
  •    DRX-600 Magnet
  •    DRX-600 Cockpit and Console
  •    Inova-600 Magnet
  •    Inova-600 Cockpit and Console
  •    Inova-600: Diagram of Cryogenic Probe System
  •    Inova-600 Cold Head with Sides Removed
  •    Inova-600 Helium Compressor and Chilled Water Manifold
  •    Inova-600 Water Chiller Indoor Unit
  •    Inova-600 Water Chiller Outdoor Unit
  •    Outline: Getting an NMR Spectrum
  •    Sample Preparation
  •    Sample Depth
  •    Lock: The Deuterium Lock Feedback Loop
  •    The Deuterium Lock Channel
  •    Lock Circuit Feedback Loop
  •    Lock Display
  •    Shimming: Maximizing the Homogeneity of the Field
  •    Diagram of Z Shims and Bo Inhomogeneity
  •    Shim Hardware and Operation
  •    Interaction of Z1 and Z2 Shims
  •    Bad Z2 Shim: Sucrose 1H Spectrum
  •    FID: Free Induction Decay
  •    Receiving the FID: Analog and Digital
  •    Receiving the FID: Block Diagram
  •    FID: CHCl3/CH2Cl2, 0 to 2 9 seconds
  •    FID: CHCl3/CH2Cl2, 0 to 0 425 seconds
  •    FID: CHCl3/CH2Cl2, 0 to 36 ms
  •    Digitization of the FID
  •    Receiver Gain Optimization
  •    Quadrature Detection: The FID in Stereo
  •    Quadrature Detection: Cartoon Model
  •    Limits to Frequency: the Nyquist Theorem
  •    Limits of Digitization: the Nyquist Theorem
  •    Exceeding the Maximum: Folding or Aliasing
  •    Folding or Aliasing
  •    Two Ways to Sample the Stereo Audio FIDs
  •    Digitized FID Data (DW = 80 microseconds)
  •    FID: CHCl3/CH2Cl2, 0 to 36 ms, Analyzed
  •    The Spectral Window
  •    Spectrum: CHCl3/CH2Cl2, with MHz, Hz and ppm Scales
  •    The Spectral Window in Units of Parts per Million
  •    Acquisition Parameters: Relationship of SW, AT and NP
  •    NMR Frequency Depends on the Observe Nucleus