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Visuals for Bruker DRX-600 NMR Training Workshop Lecture III

These visuals are made from the original lecture transparencies

  •    Gradient pulse leads to twisted coherence
  •    Gradient-Enhanced HSQC: 3 gradient pulses
  •    General Setup Procedure for DRX-500
  •    Setting Up the 2D Spectral Window
  •    The 2D Spectral Window: Bruker Parameters
  •    Number of Data Points in 2D Experiment
  •    2D NMR Parameters: Bruker
  •    Menu Display after eda Command (Page 1)
  •    Menu Display after eda Command (Page 2)
  •    Data Processing in Two Dimensions
  •    Window Functions for 2D NMR: Bruker Parameters
  •    Phase Errors in Two Dimensions
  •    Interactive 2D Phase Correction
  •    Menu Display after edp Command
  •    Cholesterol 1H and 13C Spectra Arranged on x and y Axes
  •    Cholesterol 1H and 13C Spectra with Two HSQC Crosspeaks
  •    Expansion of Downfield Region: Cholesterol HSQC with 1D Spectra
  •    Cholesterol HSQC Spectrum with 1H and 13C Spectra
  •    Cholesterol HSQC Spectrum
  •    Expansion of Upfield Region: Cholesterol HSQC with 1D Spectra
  •    Edited 13C-Decoupled HSQC of Cholesterol
  •    F2 slices at carbons j, q and s of Cholesterol HSQC
  •    HSQC / HMQC and HMBC
  •    One-bond vs 2-3 bond correlations
  •    13C-decoupled HSQC of sucrose in D2O (500 MHz, gradients)
  •    HMBC of sucrose in D2O
  •    HMBC of sucrose in D2O, with overlay of HSQC spectrum
  •    HMBC of sucrose in D2O, with diagram of 2 and 3 bond correlations
  •    HMBC of sucrose in D2O: upfield region
  •    HSQC Spectrum of Product 2: Expanded Region
  •    1D 1H Spectrum of Product 2: Two expansions (overlay)
  •    HMBC Spectrum of Product 2: Expanded Region (overlay)
  •    Conformational Effects in HMBC
  •    2D-COSY (Correlation Spectroscopy)
  •    COSY and DQF-COSY
  •    Homonuclear Shift Correlation: COSY
  •    3-heptanone in CDCl3: DQF-COSY Spectrum 600 MHz
  •    3-heptanone: DQF-COSY with H1-H2 Spin System
  •    3-heptanone: DQF-COSY with H4-H5-H6-H7 Spin System
  •    3-heptanone: DQF-COSY with Assignments and Correlation Diagram
  •    3-heptanone: DQF-COSY showing artifacts
  •    DQF-COSY Spectrum of Sucrose (Full Matrix)
  •    300 MHz COSY Spectrum of Sucrose: Full Spectrum
  •    DQF-COSY Spectrum of Sucrose: H(g1) - H(g2) Crosspeak Fine Structure
  •    300 MHz COSY Spectrum of Sucrose: Upfield Region
  •    600 MHz COSY Spectrum of Sucrose: Upfield Region
  •    Double-Quantum Filtered COSY
  •    Coherence pathway selection using gradients
  •    2D-TOCSY
  •    TOCSY overview
  •    3-heptanone in CDCl3: Simulated TOCSY Spectrum
  •    3-heptanone in CDCl3: TOCSY Spectrum 72 ms mixing 600 MHz
  •    3-heptanone in CDCl3: Overlay for TOCSY Spectrum
  •    TOCSY of Heregulin-alpha
  •    2D-NOESY (Nuclear Overhauser Effect Spectroscopy)
  •    NOESY overview
  •    Gradient-Enhanced NOESY
  •    Measurement of crosspeak volumes (sucrose NOESY)
  •    NOESY Spectrum of Unknown F
  •    NOESY Correlations for Unknown F, 13C Spectrum of Unknown F
  •    2D-ROESY (Rotating Frame Overhauser Effect Spectroscopy)
  •    Maximum Theoretical Overhauser Effect
  •    The Spin-Lock
  •    ROESY Pulse Sequence Diagram
  •    ROESY of Pristimerin Oxidation Product, olefinic to upfield
  •    ROESY of Pristimerin Oxidation Product, olefinic to upfield, with Structure Diagram
  •    Pristimerin Oxidation Product Structure with Distances and 1H Spectrum